5 Hive - 5-MeO-DMT Forum

Information => Preparation and Integration => Topic started by: HumbleVoyager on June 21, 2017, 05:01:34 PM

Title: Re-Crystallization of 5-MeO-DMT HCl
Post by: HumbleVoyager on June 21, 2017, 05:01:34 PM
Just wondering if any chemistry-type people here might have some ideas on how to best do a recrystallization of 5-MeO-DMT HCl in order to remove impurities that might be present.

I have searched the web for this but haven't been able to find anything specifically about this topic.

Thanks in advance!
Title: Re: Re-Crystallization of 5-MeO-DMT HCl
Post by: Flux on July 05, 2017, 12:43:12 AM
Also curious about this process -plus and it would be great to collate the best methods and techniques in one thread here
Title: Re: Re-Crystallization of 5-MeO-DMT HCl
Post by: 3-breaths on July 09, 2017, 04:10:32 PM
*following* I'm guessing something water based.
Title: Re: Re-Crystallization of 5-MeO-DMT HCl
Post by: HumbleVoyager on July 20, 2017, 06:48:17 PM
A chemist friend has suggested the following possible solvent systems:

Quote
Pure warm anhydrous:
  • hexane
  • ethyl acetate
  • EtOH and ethyl acetate
  • H2O and acetone

Will have to try this out and report back.